Instruments
NMR data in the spectrometers can be accesed
directly from the lab's workstations for off-line processing an
plotting. User's data can also be downloaded via
sftp but only from within the Chemistry Department and a few selected University locations.
| Varian MR400 (Gallium) |
| 400 MHz (9.4 Tesla) Premium Shielded Magnet |
 |
| Two radio frequency channels |
| Antivibration legs system |
| Waveform generator for shaped pulses |
| Temperature range: -150° to 150° C |
| Pulsed Field Gradient |
| Typically used for |
| Installed: Feb 08 |
| Varian 5 mm PFG AutoX Indirect Detection probe |
| Frequency range: |
1H {15N-31P} |
| Temp range: |
-80° to +130° C |
| Sensitivity: |
1H=660:1, 13C= |
| Other features: |
auto tunable |
| Varian MR400 (Cobalt) |
| 400 MHz (9.4 Tesla) Premium Shielded Magnet |
 |
| Two radio frequency channels |
| Antivibration legs system |
| Waveform generator for shaped pulses |
| Temperature range: 25° to 150° C |
| Pulsed Field Gradient |
| Typically used for |
| Installed: Feb 08 |
| Varian 5 mm PFG AutoX Dual Broadband probe |
| Frequency range: |
1H-19F / 15N-31P |
| Temp range: |
-80° to +130° C |
| Sensitivity: |
1H=306:1, 19F=348:1, 13C=205:1, 15N=21:1, 31P=170:1 |
| Other features: |
auto tunable |
| Varian Inova 500 (Tin) |
| 500 MHz (11.7 Tesla) Oxford Magnet |
 |
| Two radio frequency channels |
| TMC antivibration system |
| Waveform generator for shaped pulses |
| Performa I, Z-axis pulsed field gradient module and automatic gradient shimming module |
| Enhanced VT unit with high-stability option and pre-conditioning unit |
| Typically used for high field proton and heteronuclear spectra and indirect detection 2D techniques. |
| Varian indirect detection probe (id, default) |
| Frequency range: |
1H{15N-31P} |
| Temp range: |
-20° to +50°C |
| Sensitivity: (5/15/06) |
1H=560, 13C=45 |
| Other features: |
Z-gradient, 5 mm |
| Varian switchable probe (sw) |
| Frequency range: |
1H-19F/15N-31P |
| Temp range: |
-100° to +150°C |
| Sensitivity: (9/11/06) |
1H=290, 13C=256 |
| Other features: |
Z-gradient, 5 mm |
| Varian Inova 400 (Zirconium) |
| 400 MHz (9.4 Tesla) Oxford Magnet |
 |
| Two radio frequency channels |
| TMC antivibration system |
| Waveform generator for shaped pulses |
| Z-axis pulsed field gradient module |
|
Enhanced VT unit with high-stability option and pre-conditioning unit |
|
Typically used for routine 1D H/C/F/P and variable temperature experiments. |
| Varian autoswitchable probe (quad, default) |
| Frequency range: |
1H/19F/13C/31P |
| Temp range: |
-20° to +80°C |
| Sensitivity: |
1H=234,
13C=142, 19F=311, 31P=102
Lineshape=0.29, 2.23, 4.47. |
| Other features: |
Z-gradient, 5 mm |
| Varian 4 nucleus Auto·nmr probe (quad4nuc) |
| Frequency range: |
1H/19F/13C/31P
|
| Temp range: |
-20° to +80°C |
| Sensitivity (nominal): |
1H=143,
13C=108, 19F=169, 31P=63 |
| Other features: |
Z-gradient, 5 mm |
| Varian Mercury 300 (Zinc) |
| 300 MHz (7.0 Tesla) Oxford Magnet |
 |
| Two radio frequency channels (1H,19F/13C,31P) |
| Variable temperature unit |
|
This is a walk-in instrument typically used for routine 1D H/C/F/P and variable temperature experiments. |
| |
| Varian autoswitchable probe (quad, default) |
| Frequency range: |
1H/19F/13C/31P |
| Temp range: |
-100° to +150°C |
| Sensitivity: |
|
| Other features: |
5 mm |
| Varian switchable probe (sw) |
| Frequency range: |
1H-19F/15N-31P |
| Temp range: |
-150° to +200°C |
| Sensitivity (nominal): |
1H=85,
13C=84, 19F=, 31P=76 |
| Other features: |
5 mm |
| Varian Mercury 200 (Scandium) |
|
200 MHz (4.7 Tesla) "R2D2" Magnet |
 |
| Two radio frequency channels |
| SMS 100 Automatic sample changer |
| Located in room A636-A |
| Used for undergraduate teaching |
| Varian switchable probe |
| Frequency range: |
1H-19F/15N-31P |
| Temp range: |
|
| Sensitivity: |
|
| Other features: |
5 mm |
| Bruker AC200/Tecmag DSPect (Calcium) |
|
200 MHz (4.7 Tesla) Magnet |
 |
|
Tecmag NTNMR software |
| Located in room 2407 |
|
Used for undergraduate teaching |
| |
| Bruker Dual probe (default) |
| Frequency range: |
1H/13C |
| Temp range: |
|
| Sensitivity: |
|
| Other features: |
5 mm |
| Bruker Broadband probe |
| Frequency range: |
1H/109Ag-31P |
| Temp range: |
|
| Sensitivity: |
|
| Other features: |
10 mm |
Data stations
Five Dell Precision 370 computers, 3.6 GHz with Red Hat Enterprise Linux and VNMRJ LX 1.1D and 2.2C.
Varian NMRS 600 MHz Solid State
To be installed (hopefully) August/September 2008
SQUID MPMS magnetometer
The SQUID ( Superconducting QUantum
Interference Device)
is located in Chemistry Room 3411c. This system is known as
a MPMS ( Magnetic Property
Measurement System),
with a SQUID detector. Manufactured by Quantum Design www.qdusa.com
The DC magnetic field can be run from: -55,000 to 55,000 Gauss (-5.5 to
5.5 Tesla).
The sample temperature can be run from: 1.7 to 400 Kelvin (°K)
(-271.6 to 126.7 °C).
For questions contact Chris Kojiro.
Squid
operating instructions [Adobe Acrobat Reader "pdf" file]
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